Category:OSWa6c6b673d314531e83bce1010db7a848: Difference between revisions

From Battery Knowledge Base
elaborate on mixing steps
(add BattINFO links to slurry components)
(elaborate on mixing steps)
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=== Preparation ===
=== Preparation ===


* '''Weighing''': Accurately measure all components based on the desired electrode composition.
* '''Weighing''': This step involves precisely measuring each component of the slurry to match the desired electrode composition. Accurate weighing ensures the correct ratio of active materials, conductive additives, binders, and solvents, which is crucial for the performance and consistency of the final battery.
* '''Pre-mixing''': Pre-mix dry powders (active material and conductive additives) to ensure uniform distribution.
* '''Pre-mixing''': Before adding any liquids, the dry powders (active materials and conductive additives) are pre-mixed. This helps in achieving a uniform distribution of particles, preventing segregation, and ensuring that all subsequent mixing steps result in a homogenous slurry.


=== Dispersion ===
=== Dispersion ===


* '''Add Solvent''': Gradually add the solvent to the pre-mixed dry powders while stirring at a low speed to avoid agglomeration.
* '''Add Solvent''': The solvent is added gradually to the pre-mixed dry powders while stirring at a low speed. This careful addition prevents the formation of agglomerates, which are clumps of particles that can affect the uniformity and performance of the slurry.
* '''High-speed Mixing''': Use high-shear mixers or ball mills to break down agglomerates and ensure even distribution of particles. This step typically lasts several hours.
* '''High-speed Mixing''': Using high-shear mixers or ball mills, the slurry is mixed at high speeds to break down any remaining agglomerates. This step, which can take several hours, ensures that the particles are evenly distributed throughout the mixture, resulting in a smooth and consistent slurry.


=== Binder Addition ===
=== Binder Addition ===


* '''Slow Addition''': Add the binder slowly to the slurry while mixing to prevent clumping.
* '''Slow Addition''': The binder is added slowly to the slurry while continuously mixing. Adding the binder gradually helps prevent clumping, ensuring that the binder is evenly distributed throughout the slurry.
* '''High-shear Mixing''': Continue high-shear mixing until the binder is fully dissolved and evenly distributed.
* '''High-shear Mixing''': After adding the binder, high-shear mixing continues to ensure that the binder is fully dissolved and homogeneously mixed. This step is critical for the mechanical stability and adhesion properties of the final electrode.


=== Homogenization ===
=== Homogenization ===


* '''Vacuum Deaeration''': Remove air bubbles from the slurry using a vacuum to prevent defects in the coated electrodes.
* '''Vacuum Deaeration''': Air bubbles trapped in the slurry can cause defects in the coated electrodes. Vacuum deaeration removes these bubbles by applying a vacuum to the slurry, ensuring a defect-free coating process.
* '''Final Mixing''': Conduct a final mixing phase at moderate speed to ensure a homogeneous mixture.
* '''Final Mixing''': The slurry undergoes a final mixing phase at a moderate speed. This ensures that the mixture is completely homogeneous, with all components evenly distributed, ready for the coating process on the current collector.


== Equipment ==
== Equipment ==
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